Hydrazine hydrate (1:1) → HCID 67365755, compound

HRID 2243956Notes

Reaction equation

HRID 2243956 reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[C:3](=O)[C:2]2=O.COP([CH2:16][C:17]([C:19]1[CH:20]=[N:21][N:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:23]=1[CH:24]1[CH2:26][CH2:25]1)=O)(=O)OC.O.[NH2:32][NH2:33]>>[C:27]([N:22]1[C:23]([CH:24]2[CH2:26][CH2:25]2)=[C:19]([C:17]2[CH:16]=[C:3]3[C:2]([CH:1]4[CH2:7][CH:4]3[CH2:5][CH2:6]4)=[N:33][N:32]=2)[CH:20]=[N:21]1)([CH3:30])([CH3:29])[CH3:28]

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 138696Bicyclo(2.2.1)heptane-2,3-dioneHCID 86609930HCID 86609930, compound

Product 1

HCID 67365755HCID 67365755, compound

Procedure

off-white solid. MS (ESI): 309.1 (MH+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(1-tert-Butyl-5-cyclopropyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-af48a210675e409790301903cd72cf3a
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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