Hydrazine hydrate (1:1) → HCID 67364894, compound

HRID 2243962Notes

Reaction equation

HRID 2243962 reaction equation
[CH3:1][C@@:2]12[C:8]([CH3:10])([CH3:9])[C@@H:5]([CH2:6][CH2:7]1)[C:4](=O)[C:3]2=O.COP([CH2:19][C:20]([CH:22]1[CH2:25][CH2:24][CH2:23]1)=O)(=O)OC.O.[NH2:27][NH2:28]>>[CH:22]1([C:20]2[CH:19]=[C:4]3[C:3]([C@:2]4([CH3:1])[C:8]([CH3:10])([CH3:9])[C@H:5]3[CH2:6][CH2:7]4)=[N:28][N:27]=2)[CH2:25][CH2:24][CH2:23]1

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 1549179(+)-CamphorquinoneHCID 22768687Dimethyl (2-cyclobutyl-2-oxoethyl)phosphonate

Product 1

HCID 67364894HCID 67364894, compound

Procedure

light yellow solid. MS (EI): 242.2 (M+). Prepared from (1S,4R)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2,3-dione, (2-Cyclobutyl-2-oxo-ethyl)-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-347217a0f21e4c9db8e70161cab2915b
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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