Hydrazine hydrate (1:1) → HCID 16063747, compound

HRID 2243964Notes

Reaction equation

HRID 2243964 reaction equation
[CH3:1][C:2]1([CH3:9])[CH2:6][C:5](=O)[C:4](=O)[CH2:3]1.COP([CH2:16][C:17]([C:19]1[CH:20]=[N:21][N:22]([C:25]([CH3:28])([CH3:27])[CH3:26])[C:23]=1[CH3:24])=O)(=O)OC.O.[NH2:30][NH2:31]>>[C:25]([N:22]1[C:23]([CH3:24])=[C:19]([C:17]2[N:31]=[N:30][C:4]3[CH2:3][C:2]([CH3:9])([CH3:1])[CH2:6][C:5]=3[CH:16]=2)[CH:20]=[N:21]1)([CH3:28])([CH3:27])[CH3:26]

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 142896544,4-Dimethylcyclopentane-1,2-dioneHCID 86609929HCID 86609929, compound

Product 1

HCID 16063747HCID 16063747, compound

Procedure

yellow crystalline solid. MS (ESI): 285.1 (MH+). Prepared from 4,4-dimethyl-cyclopentane-1,2-dione, [2-(1-tert-Butyl-5-methyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-20e237b91da64240ba128a07b7f9eb94
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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