Hydrazine hydrate (1:1) → HCID 67365484, compound

HRID 2243969Notes

Reaction equation

HRID 2243969 reaction equation
[CH3:1][C@@:2]12[C:8]([CH3:10])([CH3:9])[C@@H:5]([CH2:6][CH2:7]1)[C:4](=O)[C:3]2=O.COP([CH2:19][C:20]([C:22]1[C:23]([CH3:34])=[N:24][N:25]([CH2:27][C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[CH:26]=1)=O)(=O)OC.O.[NH2:36][NH2:37]>>[CH2:27]([N:25]1[CH:26]=[C:22]([C:20]2[CH:19]=[C:4]3[C:3]([C@:2]4([CH3:1])[C:8]([CH3:10])([CH3:9])[C@H:5]3[CH2:6][CH2:7]4)=[N:37][N:36]=2)[C:23]([CH3:34])=[N:24]1)[C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 1549179(+)-CamphorquinoneHCID 86609936HCID 86609936, compound

Product 1

HCID 67365484HCID 67365484, compound

Procedure

yellow solid. MS (ESI): 359.1 (MH+). Prepared from (1S,4R)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2,3-dione, [2-(1-Benzyl-3-methyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-a063f5fc88d949029b06b9fa45f8b46d
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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