Hydrazine hydrate (1:1) → HCID 67364682, compound

HRID 2243973Notes

Reaction equation

HRID 2243973 reaction equation
[CH3:1][C@@:2]12[C:8]([CH3:10])([CH3:9])[C@@H:5]([CH2:6][CH2:7]1)[C:4](=O)[C:3]2=O.COP([CH2:19][C:20](=O)[CH2:21][C:22]1[CH:27]=[CH:26][C:25]([Cl:28])=[CH:24][CH:23]=1)(=O)OC.O.[NH2:31][NH2:32]>>[Cl:28][C:25]1[CH:26]=[CH:27][C:22]([CH2:21][C:20]2[CH:19]=[C:4]3[C:3]([C@:2]4([CH3:1])[C:8]([CH3:10])([CH3:9])[C@H:5]3[CH2:6][CH2:7]4)=[N:32][N:31]=2)=[CH:23][CH:24]=1

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 1549179(+)-CamphorquinoneHCID 21507592Dimethyl [3-(4-chlorophenyl)-2-oxopropyl]phosphonate

Product 1

HCID 67364682HCID 67364682, compound

Procedure

light yellow oil. MS (EI): 313.2 (M+). Prepared from (1S,4R)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2,3-dione, [3-(4-Chloro-phenyl)-2-oxo-propyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-c82db339074846c086692ab8500c17c8
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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