HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl Citrate → Ethyl Acetoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl Citrate | HCID 6506 | — |
| Catalyst | Titanium isopropoxide | HCID 11026 | — |
| Product | Ethyl Acetoacetate | HCID 8868 | — |
Reaction Steps
In the same way as in Example 1, 60 g (0.21 mol) of tetraisopropyl titanate were reacted with 116.6 g (0.42 mol) of triethyl citrate. The mixture was freed of alcohol under vacuum and 154.6 g of a clear, pale yellow liquid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05428103 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-0b1f2e1c0f294ff991c72bb3ca95134c |
| Source note | uspto-grants-1995_06 |