HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86737317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 86737316 | HCID 86737316 | — |
| Product | HCID 86737317 | HCID 86737317 | — |
Reaction Steps
A mixture of 6-acetyl-2,4-bis(trichloromethylbenzo[1,3]dioxin (2.0 g.) and 100% hydrazine hydrate (0.25 g.) in absolute ethanol (25 ml.) was heated under reflux for 16 hours, and cooled to give 6-acetyl-2,4-bis(trichloromethyl)benzo[1,3]dioxin hydrazone, m.p. 159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232032 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-718d4b98a81f44c7aa217a7b4f3e1d28 |
| Source note | uspto-grants-1980_11 |