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HRID224410

反应详情

EQUATION

反应方程式

HRID 224410 的结构方程式

REACTANTS

反应物

3
结构：CCO
HCID702

Ethanol

C2H6O

结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：ClC(Cl)(Cl)C1OCc2ccccc2O1
HCID86737316

未命名化合物

PRODUCTS

生成物

1
结构：CC(=NN)c1ccc2c(c1)C(C(Cl)(Cl)Cl)OC(C(Cl)(Cl)Cl)O2
HCID86737317

未命名化合物

PROCEDURE

实验过程

A mixture of 6-acetyl-2,4-bis(trichloromethylbenzo[1,3]dioxin (2.0 g.) and 100% hydrazine hydrate (0.25 g.) in absolute ethanol (25 ml.) was heated under reflux for 16 hours, and cooled to give 6-acetyl-2,4-bis(trichloromethyl)benzo[1,3]dioxin hydrazone, m.p. 159° C.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureunder reflux for 16 hours
  3. temperaturecooled