Hydrochloric Acid → HCID 12878330, compound

HRID 224427Notes

Reaction equation

HRID 224427 reaction equation
[CH:1]1([C:7]2[CH:12]=[CH:11][C:10]([CH2:13][C:14]([OH:16])=[O:15])=[C:9]([O:17][CH3:18])[CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Cl.[CH3:20]O>>[CH3:20][O:15][C:14](=[O:16])[CH2:13][C:10]1[CH:11]=[CH:12][C:7]([CH:1]2[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]2)=[CH:8][C:9]=1[O:17][CH3:18]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 12878329(4-Cyclohexyl-2-methoxyphenyl)acetic acid

Product 1

HCID 12878330HCID 12878330, compound

Procedure

A solution of 20 g of (4-cyclohexyl-2-methoxyphenyl)-acetic acid in 200 ml of dry methanol is saturated with HCl gas at 0°. After standing at 22° for 18 hours, it is evaporated to dryness.

Workup

  1. customit is evaporated to dryness

Sources & evidence

ORD record
ord-c073d2c2636d432592dbdc3699d0d88a
Source dataset
uspto-grants-1980_11
Patent number
US04232039

Reaction notes

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