HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12878341, compound → HCID 12878342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12878341 | HCID 12878341 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12878342 | HCID 12878342 | — |
Reaction Steps
1 g of 4-hydroxy-4-(4-cyclohexyl-2-methoxyphenyl)-butyric acid is dissolved in 20 ml of ethyl acetate and hydrogenated in the presence of 100 mg of Pd on carbon (10%). When the hydrogen has been completely absorbed, filtration takes place. The filtrate is evaporated and the residue is recrystallised from CH2Cl2 -pentane. M.p. 104°-105°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232039 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-3d02b2c493fa4130baead1da5e04055c |
| Source note | uspto-grants-1980_11 |