HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23333159, compound → HCID 23333169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23333159 | HCID 23333159 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 23333169 | HCID 23333169 | — |
Reaction Steps
9.2 g of 6-cyclohexyl-3-methyl-benzofuran are dissolved in 140 ml of ethyl acetate and hydrogenated in the presence of palladium (10% on active charcoal). After 5 hours, the mixture is filtered and reduced in volume. 6-Cyclohexyl-2,3-dihydro-3-methyl-benzofuran is obtained as an oily product by distillation in a bulb tube at 120°/0.1 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232039 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-66ed1b29850847a0b92fbfc79d211974 |
| Source note | uspto-grants-1980_11 |