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HRID2244472

反应详情

EQUATION

反应方程式

HRID 2244472 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC(Oc1ccc(Cl)cc1Cc1cc(Cl)ccc1OCC(=O)OCc1ccccc1)C(=O)OC(C)(C)C
HCID68452343

未命名化合物

PRODUCTS

生成物

1
结构：CC(Oc1ccc(Cl)cc1Cc1cc(Cl)ccc1OCC(=O)OCc1ccccc1)C(=O)O
HCID68452550

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

A solution of 2-[2-(2-benzyloxycarbonylmethoxy-5-chloro-benzyl)-4-chloro-phenoxy]-propionic acid tert-butyl ester (1.736 g, 3.18 mmol) in DCM (10 mL) is treated with TFA (5 mL) and allowed to stir at RT for 1 hour. The solvent is removed in vacuo to yield the titled compound as an off-white solid.

WORKUP

后处理

  1. customThe solvent is removed in vacuo