Hydrochloric Acid → HCID 86594827, compound

HRID 2244508Notes

Reaction equation

HRID 2244508 reaction equation
O.[ClH:2].[CH3:3][N:4]([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30]/[CH:31]=[CH:32]\[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH3:40])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]/[CH:13]=[CH:14]\[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(O)C>[ClH:2].[CH3:3][N:4]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]/[CH:13]=[CH:14]\[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30]/[CH:31]=[CH:32]\[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH3:40]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 962WaterHCID 15706419(9Z)-N-Methyl-N-(9Z)-9-octadecenyl-9-octadecen-1-amine

Product 1

HCID 86594827HCID 86594827, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Conditions

Temperature
60 °C

Procedure

To 60 mL of water, 60 mL of ethanol and 2.0 mL of 37% concentrated hydrochloric acid were added, and then, 11.7 g (0.022 mol) of N-methyldioleylamine was added. The mixture was heated to 60° C. to give a solution of N-methyldioleylamine hydrochloride. To this solution, 20 g of hectolite was added. The thus-obtained slurry was stirred at 60° C. for 3 hours. The supernatant was removed, and the residual liquid was washed with 1 L of water at 60° C. and then dried at 60° C. under a pressure of 10−3 Torr for 24 hours. The dried product was pulverized by a jet mill to give a modified hectolite having an average particle diameter of 5.2 μm. Elemental analysis of the modified hectolite revealed that the amount of N-methyldioleylammonium ion was 0.85 mmol per g of the modified hectolite.

Sources & evidence

ORD record
ord-89689c148adf43338e7b2645e8c25ce0
Source dataset
uspto-grants-2010_03
Patent number
US07678866B2

Reaction notes

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