HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 54463040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 23333245 | HCID 23333245 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54463040 | HCID 54463040 | — |
Reaction Steps
6.5 g of the keto-compound of step 4 were dissolved in 90 ml of methanol and hydrogenated with a solution of 0.75 g of sodium borohydride in 8 ml of water as described for compound 17, step 5. The crude carbinol formed was recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232107 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-a233c85a4cb54d76b87318407b04cbf8 |
| Source note | uspto-grants-1980_11 |