1,2-Dichloroethane → HCID 11577035, compound

Participants

Reaction Steps

To a solution of 2-(2-methylphenyl)-2-(4-chlorophenylaminocarbonylamino)-acetic acid (from EXAMPLE 84, 40 mg, 0.13 mmol) and 4-(4-methyl-homopiperazinyl)phenylamine (61 mg, 0.25 mmol) in DMF (3 mL) and H2O (1 mL), EDC (96 mg, 0.50 mmol) was added. After being stirred at room temperature for 2 h, the mixture was concentrated in vacuo. The residue was purified by HPLC to give the titled compound as a powder (25 mg). MS 506.2 and 508.2 (M+H, Cl pattern).

Provenance & Evidence