HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 54247646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | HCID 2771921 | HCID 2771921 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54247646 | HCID 54247646 | — |
Reaction Steps
The procedure of Example Ib was followed using 8 g. of the 5-(1-phenoxypropyl)-2-amino-1,3,4-thiadiazole (prepared above) and 100 ml. of ethylacetate saturated with phosgene. Topping and removing of the phosgene resulted in a glassy, orange residue of 5-(1-phenoxypropyl)-1,3,4-thiadiazol-2-yl isocyanate dimer (10.9 grams).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04233057 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-dda3619240144b5bb504e8c3301fcb05 |
| Source note | uspto-grants-1980_11 |