Methyl p-toluenesulfonate → HCID 86615029, compound

HRID 2245290Notes

Reaction equation

HRID 2245290 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[N:5][C:6]2[C:11]([CH:12]=1)=[C:10]([N+:13]([O-:15])=[O:14])[CH:9]=[CH:8][CH:7]=2.[CH3:16][C:17]1[CH:22]=[CH:21][C:20]([S:23]([O:26]C)(=[O:25])=[O:24])=[CH:19][CH:18]=1>C(#N)C>[CH3:16][C:17]1[CH:18]=[CH:19][C:20]([S:23]([O-:26])(=[O:25])=[O:24])=[CH:21][CH:22]=1.[CH3:1][O:2][C:3]1[CH:4]=[N+:5]([CH3:16])[C:6]2[C:11]([CH:12]=1)=[C:10]([N+:13]([O-:15])=[O:14])[CH:9]=[CH:8][CH:7]=2

Participants

4

Reactant 2

HCID 6645Methyl p-toluenesulfonateHCID 59216593HCID 59216593, compound

Product 1

HCID 86615029HCID 86615029, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

A mixture of 3-methoxy-5-nitroquinoline and methyl 4-methylbenzenesulfonate in acetonitrile is refluxed. After cooling, the precipitate is collected by filtration to provide 3-methoxy-1-methyl-5-nitroquinolinium 4-methylbenzenesulfonate.

Workup

  1. temperatureis refluxed
  2. temperatureAfter cooling
  3. filtrationthe precipitate is collected by filtration

Sources & evidence

ORD record
ord-7958c940444943658df7a3fb9866c29c
Source dataset
uspto-grants-2010_03
Patent number
US07683076B2

Reaction notes

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