HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59216591, compound → HCID 59216602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59216591 | HCID 59216591 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59216602 | HCID 59216602 | — |
Reaction Steps
A mixture of 1-methyl-5-nitro-1,4-dihydroquinolin-3(2H)-one and catalytic amount of palladium on carbon in methanol is stirred under hydrogen for 3 hours. The resulting mixture is filtered through a pad of celite, and the filtrate is concentrated under reduced pressure to afford 5-amino-1-methyl-1,4-dihydroquinolin-3(2H)-one
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07683076B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-fe41448562874321b0dbfb723894ec74 |
| Source note | uspto-grants-2010_03 |