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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2245345Generated: October 31, 2026

Dichloromethane → HCID 68687298, compound

https://huagongshe.com/reaction/2245345

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantTriethylamineHCID 8471—
ReactantHCID 58745477HCID 58745477—
ProductHCID 68687298HCID 68687298—

Reaction Steps

(3R,4S)-4-Amino-piperidine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester (540 mg, synthesized according to Duan, Jingwu et al, PCT Int. Appl. (2001), WO 2001070673 A2) and WO 2002002525) was dissolved in abs. DCM and NEt3 (0.39 ml) was added.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07683079B2
Source datasetuspto-grants-2010_03
ORD IDord-54a6637751ed42aeb3c2f4876f8ef097
Source noteuspto-grants-2010_03