3-Phenylprop-2-Enal → HCID 23331258, compound

HRID 224541Notes

Reaction equation

C(C=C)=O.C(=O)C=CC1C=CC=CC=1.C(=O)/C=C/C.C(SC(C)C=O)CCCCCCCCCCC.[CH2:37]([S:49][CH:50]([CH2:53][C:54]1C=CC=CC=1)[CH:51]=[O:52])[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH3:48]>>[CH2:37]([S:49][CH:50]([CH2:53][CH3:54])[CH:51]=[O:52])[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH3:48]

Participants

Reactant 5

HCID 3073-Phenylprop-2-Enal

HCID 7847Acrolein

HCID 447466Crotonaldehyde

HCID 23331262HCID 23331262, compound

HCID 23331263HCID 23331263, compound

Product 1

HCID 23331258HCID 23331258, compound

Procedure

If in the above reaction acrolein or cinnamaldehyde are used in place of crotonaldehyde, n-dodecylthiopropanal and n-dodecylthio-3-phenylpropanal respectively are obtained.

Workup

customrespectively are obtained

Sources & evidence

ORD record: ord-b5484cfc768e4ba4975c2e9b13d2f955
Source dataset: uspto-grants-1980_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04233209

Reaction notes

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