HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10214443, compound → HCID 135514435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10214443 | HCID 10214443 | — |
| Reactant | HCID 85873132 | HCID 85873132 | — |
| Product | HCID 135514435 | HCID 135514435 | 12% |
Reaction Steps
The title compound was prepared as described for Example 101 using 4-[(6-chloro-1-oxidopyridin-3-yl)methyl]morpholine and N-methyl-2-oxoindoline-5-carboxamide. Yield: 12%: 1H NMR (D2O, 400 MHz) δ 7.82 (d, J=2 Hz, 1H), 7.58 (dd, J=9, 2 Hz, 1H), 7.45 (br s, 1H), 7.28 (m, 2H), 6.92 (d, J=8 Hz, 1H), 4.16 (s, 2H), 4.12 (m, 2H), 3.79 (m, 2H), 3.46 (m, 2H), 3.24 (m, 2H), 2.90 (s, 3H); MS (TSP) m/z 367 (M++1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07683067B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-a39319fa89d74b579f6efb801cf37488 |
| Source note | uspto-grants-2010_03 |