HRID224568
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Into a 300 ml. flask equipped with mechanical stirrer and a condenser, and maintained under a nitrogen atmosphere, were added 21.5 grams magnesium acetate tetrahydrate and 100 ml. acetic anhydride and the mixture was heated at the reflux temperature for 3 hours. After the mixture had cooled, the liquid was drawn off and the solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours to obtain anhydrous magnesium acetate.
WORKUP
后处理
- customflask equipped with mechanical stirrer and a condenser
- temperaturemaintained under a nitrogen atmosphere
- temperatureAfter the mixture had cooled
- dry with materialthe solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours