HRID224568

反应详情

EQUATION

反应方程式

HRID 224568 的结构方程式

PROCEDURE

实验过程

Into a 300 ml. flask equipped with mechanical stirrer and a condenser, and maintained under a nitrogen atmosphere, were added 21.5 grams magnesium acetate tetrahydrate and 100 ml. acetic anhydride and the mixture was heated at the reflux temperature for 3 hours. After the mixture had cooled, the liquid was drawn off and the solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours to obtain anhydrous magnesium acetate.

WORKUP

后处理

  1. customflask equipped with mechanical stirrer and a condenser
  2. temperaturemaintained under a nitrogen atmosphere
  3. temperatureAfter the mixture had cooled
  4. dry with materialthe solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours