HRID224569
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Into a 300 ml. flask equipped as in EXAMPLE I and maintained under a nitrogen atmosphere were added 21.5 grams magnesium acetate tetrahydrate and 80 ml. acetic anhydride and the mixture was heated at the reflux temperature for 1 hour. After cooling, a clear liquid was drawn off and the remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours to obtain anhydrous magnesium acetate.
WORKUP
后处理
- customflask equipped as in EXAMPLE I
- temperaturemaintained under a nitrogen atmosphere
- temperatureAfter cooling
- dry with materialthe remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours