HRID224569

反应详情

EQUATION

反应方程式

HRID 224569 的结构方程式

PROCEDURE

实验过程

Into a 300 ml. flask equipped as in EXAMPLE I and maintained under a nitrogen atmosphere were added 21.5 grams magnesium acetate tetrahydrate and 80 ml. acetic anhydride and the mixture was heated at the reflux temperature for 1 hour. After cooling, a clear liquid was drawn off and the remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours to obtain anhydrous magnesium acetate.

WORKUP

后处理

  1. customflask equipped as in EXAMPLE I
  2. temperaturemaintained under a nitrogen atmosphere
  3. temperatureAfter cooling
  4. dry with materialthe remaining solid was dried at 35° C. under a vacuum of 0.3 mm mercury for several hours