HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 54703139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54703406 | HCID 54703406 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54703139 | HCID 54703139 | 81.3% |
Reaction Steps
14.5 gm (50 millimols) of methyl 6-chloro-4-hydroxy-2H-1,2-benzothiazine-3-carboxylate-1,1-dioxide were reacted with 21.3 gm (150 millimols) of methyl iodide and 50 ml of 1N sodium hydroxide in 165 ml of methanol, yielding 12.35 gm (81% of theory) of methyl 6-chloro-4-hydroxy-2-methyl-2H-1, 2-benzothiazine-3-carboxylate-1,1-dioxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04233299 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-3acd6f6cbf604ffcb17e6f07fe7ca451 |
| Source note | uspto-grants-1980_11 |