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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2246062Generated: November 3, 2026

Triphenylphosphine → HCID 10207804, compound

https://huagongshe.com/reaction/2246062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriphenylphosphineHCID 11776—
ReactantDiisopropyl azodicarboxylateHCID 5363146—
ReactantHCID 53715168HCID 53715168—
ReactantHCID 67159504HCID 67159504—
SolventTolueneHCID 1140—
ProductHCID 10207804HCID 10207804—

Reaction Steps

reaction of 1-[bis(4-chlorophenyl)methyl]azetidin-3-ol hydrobromide with N-quinolin-6-ylmethanesulfonamide in the presence of DIAD and triphenylphosphine in toluene, to form N-{1-[bis(4-chlorophenyl)methyl]azetidin-3-yl}-N-quinol-6-yl-methylsulfonamide (the reaction is preferably performed at a temperature of between 40 and 60° C.), and then

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07687493B2
Source datasetuspto-grants-2010_03
ORD IDord-9622cd16fef84ac38b55ca7256e51d5c
Source noteuspto-grants-2010_03