反应详情

A solution of Compound 3 (200 mg) and sodium iodide (200 mg) in 2-butanone (4 mL) was heated at 80° C. for 24 hours. Solvent was removed under reduced pressure and directly purified on a silica gel using 1% ethanol in dichloromethane to obtain the required product in 85% yield (200 mg).

1. customSolvent was removed under reduced pressure
2. customdirectly purified on a silica gel using 1% ethanol in dichloromethane