HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxypyridine → HCID 25260922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxypyridine | HCID 74201 | — |
| Reactant | HCID 25260767 | HCID 25260767 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 25260922 | HCID 25260922 | 60% |
Reaction Steps
A solution of Compound 12 (60 mg) and 2-methoxypyridine (0.1 mL) in N,N-dimethylformamide (1 mL) was heated at 70° C. for 16 hours. The reaction mixture was concentrated under vacuum and the residue was directly eluted on a silica gel column using 4% ethanol in dichloromethane to obtain the required product in 60% yield (34 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687496B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-82c0a5bf5f8b49ceb27f0ee0055202fb |
| Source note | uspto-grants-2010_03 |