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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2246538Generated: November 3, 2026

2-Methoxypyridine → HCID 25260922, compound

https://huagongshe.com/reaction/2246538

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethoxypyridineHCID 74201—
ReactantHCID 25260767HCID 25260767—
SolventDimethylformamideHCID 6228—
ProductHCID 25260922HCID 2526092260%

Reaction Steps

A solution of Compound 12 (60 mg) and 2-methoxypyridine (0.1 mL) in N,N-dimethylformamide (1 mL) was heated at 70° C. for 16 hours. The reaction mixture was concentrated under vacuum and the residue was directly eluted on a silica gel column using 4% ethanol in dichloromethane to obtain the required product in 60% yield (34 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07687496B2
Source datasetuspto-grants-2010_03
ORD IDord-82c0a5bf5f8b49ceb27f0ee0055202fb
Source noteuspto-grants-2010_03