Trimethyl phosphite → HCID 25262631, compound

Participants

Reaction Steps

A solution of Compound 12 (60 mg) in trimethyl phosphite (1 mL) was heated under argon at 80° C. for 10 hours. Trimethyl phosphite was removed from the reaction mixture under vacuum and the residue was eluted on a silica gel using 4% ethanol in dichloromethane to obtain the required product in 76% yield (44 mg).

Provenance & Evidence