Ethanol → HCID 74438044, compound

Participants

Reaction Steps

A mixture of Compound 53 (20 mg, 0.027 mmol), 10% palladium on carbon (4 mg, 20%) in 1 mL of ethanol was hydrogenated for 17 hours at a balloon pressure of hydrogen at 21° C. The catalyst was removed by filtration over celite and the filtrate was evaporated to give a crude product, which was chromatographed to give the desired product.

Provenance & Evidence