HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 23331741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 23331782 | HCID 23331782 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 23331741 | HCID 23331741 | 34% |
Reaction Steps
In 1,2-dichloroethane, 2-(2,5-dimethylpyrrol-1-yl)ethyl acetate was reacted with p-chlorobenzoyl chloride in the presence of aluminum chloride at room temperature for 18 hours to afford compound (340) in a yield of 34.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04233309 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-ba80f5dd979d4d7b85a92d166cb44575 |
| Source note | uspto-grants-1980_11 |