HRID2246642

反应详情

EQUATION

反应方程式

HRID 2246642 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of ethyl 3-(4-(benzyloxy)phenyl)-3-(5-methyloxazol-2-yl)propanoate (M5.3) (2.47 mmol) and Pd—C (270 mg) in EtOH was stirred under hydrogen atmosphere at room temperature for 4 hours. The Pd—C was removed by filtration through silica gel eluting with EtOH. After concentration, product M5 was obtained. MS ESI (pos.) m/e 276 (M+H).

WORKUP

后处理

  1. customThe Pd—C was removed by filtration through silica gel eluting with EtOH
  2. concentrationAfter concentration, product
  3. customwas obtained