HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57835837, compound → HCID 57835847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57835837 | HCID 57835837 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57835847 | HCID 57835847 | — |
Reaction Steps
A mixture of ethyl 3-(4-(benzyloxy)phenyl)-3-(5-methyloxazol-2-yl)propanoate (M5.3) (2.47 mmol) and Pd—C (270 mg) in EtOH was stirred under hydrogen atmosphere at room temperature for 4 hours. The Pd—C was removed by filtration through silica gel eluting with EtOH. After concentration, product M5 was obtained. MS ESI (pos.) m/e 276 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687526B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-9cb2728320294b9fb763cd9c05e3268c |
| Source note | uspto-grants-2010_03 |