HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 16067642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 68523673 | HCID 68523673 | — |
| Reactant | HCID 68525657 | HCID 68525657 | — |
| Product | HCID 16067642 | HCID 16067642 | — |
Reaction Steps
In an analogous manner to Example 14, step 3 1-cyclopropyl-3-[(1S)-3-(methylamino)-1-phenylpropyl]-1,3-dihydro-2H-benzimidazol-2-one HCl salt as a yellow amorphous solid was prepared from 1-cyclopropyl-3-[(1S)-3-(chloro)-1-phenylpropyl]-1,3-dihydro-2H-benzimidazol-2-one and methylamine. MS (ESI) m/z 322. HRMS: calculated for C20H23N3O+H+, 322.19139; found (ESI, [M+H]+), 322.192.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687529B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-e5bc40e7a5454fb7a64b601c7f5e6bb9 |
| Source note | uspto-grants-2010_03 |