HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hexyl-2-methoxy-1-phenoxybenzene → 2-Methoxy-4-octyl-1-phenoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hexyl-2-methoxy-1-phenoxybenzene | HCID 68425585 | — |
| Reactant | HCID 178443579 | HCID 178443579 | — |
| Reactant | HCID 178444611 | HCID 178444611 | — |
| Product | 2-Methoxy-4-octyl-1-phenoxybenzene | HCID 68423659 | — |
Reaction Steps
The procedure as described above for synthesis of (4a) was used, except that hexyl magnesium chloride was replaced with octyl magnesium chloride. 1H NMR (300 MHz) (CDCl3): δ 7.36-6.90 (m, 8H), 3.90 (s, 3H), 2.69-2.65 (t, 2H), 1.72-1.68 (m, 2H), 1.42-1.36 (m, 10H), 1.00-0.94 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687547B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-e94fd878183243a2b79542fa9f100779 |
| Source note | uspto-grants-2010_03 |