HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hexyl-2-phenoxyphenol → 5-Octyl-2-phenoxyphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hexyl-2-phenoxyphenol | HCID 5274977 | — |
| Reactant | 2-Methoxy-4-octyl-1-phenoxybenzene | HCID 68423659 | — |
| Reactant | 4-Hexyl-2-methoxy-1-phenoxybenzene | HCID 68425585 | — |
| Product | 5-Octyl-2-phenoxyphenol | HCID 5274979 | — |
Reaction Steps
The procedure as described above for synthesis of (5a) was used, except that compound (4a) was replaced with compound (4b). 1H NMR (300 MHz) (CDCl3) δ 7.43-6.72 (m, 8H), 5.58 (s, 1H), 2.66-2.61 (t, 2H), 1.71-1.66 (m, 2H), 1.39-1.35 (m, 10H), 0.99-0.95 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687547B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-4396f75bce7949e8aeaae66ff71e9609 |
| Source note | uspto-grants-2010_03 |