Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Nitroaniline | HCID 7423 | — |
| Reactant | 2,2-Dichloro-1,4-dioxane | HCID 12424325 | — |
| Product | HCID 17982613 | HCID 17982613 | — |
Reaction Steps
A mixture of 1.12 g (8.12 mmol) of 3-nitroaniline and 1.11 g of 2-chlorodioxene (contains 6% of 2,2-dichlorodioxane) is heated at 80° C. with stirring for 24 hours, giving 2.1 g of 2-(2-chloroethoxy)-N-(3-nitrophenyl)acetamide as brownish oil. ESI 259.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07687624B2 |
|---|
| Source dataset | uspto-grants-2010_03 |
|---|
| ORD ID | ord-7276bebf351b48c0b460821d6daf6baa |
|---|
| Source note | uspto-grants-2010_03 |
|---|
