HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 11281969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 10364769 | HCID 10364769 | — |
| Product | HCID 11281969 | HCID 11281969 | 37% |
Reaction Steps
The title compound was prepared by reacting (S)-N-[3-{4-[4-carboethoxymethylidenepiperidin-1-yl]-3-fluorophenyl}-2-oxo-1,3-oxazolidin-5-ylmethyl]-acetamide (0.3 mmol) and m-chloroperbenzoic acid (0.31 mmol) in dichloromethane at a temperature 0° C. for 14 hours in 37% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687627B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-8438ccf650fc42d0b474bb83fe2c7591 |
| Source note | uspto-grants-2010_03 |