HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Dimethylamino)ethanol → HCID 23330312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 23330312 | HCID 23330312 | — |
Reaction Steps
270 mg of 2-dimethylaminoethanol in 5 ml of acetonitrile are stirred with 630 mg of chloroformic acid p-nitrophenyl ester at room temperature for 30 minutes, the mixture is concentrated in vacuo and the residue is stirred with 2 ml of ethyl acetate; yield: 0.4 g; IR: 1770 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234572 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-a6d61409dcb9419c80f69d0aedd5f4cc |
| Source note | uspto-grants-1980_11 |