HRID2247695

反应详情

EQUATION

反应方程式

HRID 2247695 的结构方程式

PROCEDURE

实验过程

The title compound (1.1 g) was synthesized in a yield of 93% as a white crystalline solid by conducting a reaction similar to that mentioned in Example 10 (10e) using 3,4-difluorobenzaldehyde (0.71 g, 5.0 mmol), phenol (0.56 g, 6.0 mmol), potassium carbonate (1.4 g, 10 mmol), 2-methyl-2-butene (2.5 mL, 23 mmol), potassium dihydrogenphosphate (1.6 g, 12 mmol), and sodium hypochlorite (1.3 g, 14 mmol).

WORKUP

后处理

  1. customa reaction similar to