2-Methyl-2-butene → HCID 63037963, compound

Participants

Reaction Steps

The title compound (2.2 g) was synthesized in a yield of 94% as a white crystalline solid by conducting the similar reaction to that mentioned in Example 10 (10e) using 4-fluorobenzaldehyde (1.3 g, 10 mmol), 2,3-difluorophenol (2.0 g, 15 mmol), potassium carbonate (2.8 g, 20 mmol), 2-methyl-2-butene (4.9 ml, 46 mmol), potassium dihydrogenphosphate (3.1 g, 23 mmol) and sodium hypochlorite (2.5 g, 27 mmol).

Provenance & Evidence