2-Methyl-2-butene → HCID 63037963, compound

HRID 2247719Notes

Reaction equation

HRID 2247719 reaction equation
F[C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][CH:3]=1.[F:10][C:11]1[C:16]([F:17])=[CH:15][CH:14]=[CH:13][C:12]=1[OH:18].C(=O)([O-])[O-:20].[K+].[K+].CC(=CC)C.P([O-])(O)(O)=O.[K+].Cl[O-].[Na+]>>[F:10][C:11]1[C:16]([F:17])=[CH:15][CH:14]=[CH:13][C:12]=1[O:18][C:2]1[CH:9]=[CH:8][C:5]([C:6]([OH:20])=[O:7])=[CH:4][CH:3]=1

Participants

7

Reactant 6

HCID 105532-Methyl-2-buteneHCID 11430Potassium CarbonateHCID 680234-FluorobenzaldehydeHCID 808792,3-DifluorophenolHCID 516951Monobasic potassium phosphateHCID 23665760Sodium Hypochlorite

Product 1

HCID 63037963HCID 63037963, compoundYield 94%

Procedure

The title compound (2.2 g) was synthesized in a yield of 94% as a white crystalline solid by conducting the similar reaction to that mentioned in Example 10 (10e) using 4-fluorobenzaldehyde (1.3 g, 10 mmol), 2,3-difluorophenol (2.0 g, 15 mmol), potassium carbonate (2.8 g, 20 mmol), 2-methyl-2-butene (4.9 ml, 46 mmol), potassium dihydrogenphosphate (3.1 g, 23 mmol) and sodium hypochlorite (2.5 g, 27 mmol).

Workup

  1. customthe similar reaction to

Sources & evidence

ORD record
ord-4fc51c7dc4b847358f85748494620691
Source dataset
uspto-grants-2010_03
Patent number
US07687491B2

Reaction notes

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