Hydrochloric Acid → HCID 178479427, compound

HRID 2247822Notes

Reaction equation

HRID 2247822 reaction equation
[NH:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]/[C:12]([OH:14])=[O:13])[C:2]([NH2:4])=[NH:3].[ClH:15]>>[ClH:15].[NH:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]/[C:12]([OH:14])=[O:13])[C:2]([NH2:4])=[NH:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178512799HCID 178512799, compound

Product 1

HCID 178479427HCID 178479427, compound

Procedure

A suspension of 13 g (65 mmoles) of crude (11) in 75 mL lN hydrochloric acid was warmed on a steam bath until a clear solution was obtained. After 1 h at room temperature crystals were noted. The mixture was chilled overnight and the crystals were filtered and dried to provide 13.86 g of title compound (12), mp 162° C. Anal. Calcd. for C9H18N3O2Cl: C, 45.86; H, 7.70; N, 17.83; Cl, 15.04. Found: C, 45.90; H, 7.64; N, 17.88; Cl, 14.79.

Workup

  1. temperaturewas warmed on a steam bath until a clear solution
  2. customwas obtained
  3. temperatureThe mixture was chilled overnight
  4. filtrationthe crystals were filtered
  5. customdried

Sources & evidence

ORD record
ord-58599f6fc95d4de2aafafc2e3811a96b
Source dataset
uspto-grants-1991_08
Patent number
US05037808

Reaction notes

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