HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenyl-2-(triphenylphosphoranylidene)ethanone → HCID 54417837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenyl-2-(triphenylphosphoranylidene)ethanone | HCID 70073 | — |
| Reactant | 5-Formylthiophene-2-Carbonitrile | HCID 12280004 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54417837 | HCID 54417837 | 56.6% |
Reaction Steps
A mixture of 2-cyano-5-formylthiophene (4 g) and benzoylmethylenetriphenylphosphorane (11.09 g) in tetrahydrofuran (40 ml) was refluxed for 30 minutes. The reaction mixture was evaporated in vacuo to give 3-(5-cyano-2-thienyl)-1-phenyl-2-propen-1-one (3.95 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05037824 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-44df1a27d69f4d52a86eab8cd1706fd8 |
| Source note | uspto-grants-1991_08 |