1,12-Dodecanediamine → HCID 18644959, compound

HRID 2248068Notes

Reaction equation

HRID 2248068 reaction equation
[CH2:1]([OH:24])[C@H:2]1[O:7][C@H:6]([O:8][CH2:9][C@@H:10]([OH:20])[C@@H:11]([OH:19])[C@H:12]([OH:18])[C@@H:13]([OH:17])[C:14](O)=[O:15])[C@H:5]([OH:21])[C@@H:4]([OH:22])[C@H:3]1[OH:23].[NH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][NH2:38]>>[CH2:37]([NH:38][C:14]([C@@H:13]([C@H:12]([C@@H:11]([C@@H:10]([CH2:9][O:8][C@H:6]1[O:7][C@H:2]([CH2:1][OH:24])[C@H:3]([OH:23])[C@H:4]([OH:22])[C@H:5]1[OH:21])[OH:20])[OH:19])[OH:18])[OH:17])=[O:15])[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][NH:25][C:14]([C@@H:13]([C@H:12]([C@@H:11]([C@@H:10]([CH2:9][O:8][C@H:6]1[O:7][C@H:2]([CH2:1][OH:24])[C@H:3]([OH:23])[C@H:4]([OH:22])[C@H:5]1[OH:21])[OH:20])[OH:19])[OH:18])[OH:17])=[O:15]

Participants

3

Reactant 2

HCID 177271,12-DodecanediamineHCID 1935746-O-Hexopyranosylhexonic acid

Product 1

HCID 18644959HCID 18644959, compoundYield 75.1%

Procedure

3.96 g of potassium melibionate (Sigma Chemie) are reacted with 1.00 g of 1,12-diaminododecane analogously to Example 3 and 3.3 g of the title compound are obtained.

Sources & evidence

ORD record
ord-19e9476cd90a4bfe9871d83b445b2c34
Source dataset
uspto-grants-1991_08
Patent number
US05037973

Reaction notes

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