HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 15662548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 11435274 | HCID 11435274 | — |
| Product | HCID 15662548 | HCID 15662548 | — |
Reaction Steps
Chloroacetone (0.89 ml, 1.04 g, 11.2 mmol) is added to a mixture of 4-(3-methyl-2-butenoxy)phenol (2.0 g, 11.2 mmol), potassium carbonate (25 g) and potassium iodide (2.6 g) in 125 mol of anhydrous acetone. The mixture is heated under reflux for 4.5 hours and then is allowed to cool to RT to give 4-(3-methyl-2-butenoxy)phenoxyacetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05037991 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-656ebda34227434cbe3032fad8c5a86a |
| Source note | uspto-grants-1991_08 |