Ethyl isothiocyanate → HCID 19816552, compound

HRID 2248165Notes

Reaction equation

HRID 2248165 reaction equation
[CH3:1][C:2]([CH3:16])=[CH:3][CH2:4][O:5][C:6]1[CH:15]=[CH:14][C:9]([O:10][CH2:11][CH2:12][OH:13])=[CH:8][CH:7]=1.[H-].[Na+].[CH2:19]([N:21]=[C:22]=[S:23])[CH3:20]>>[CH2:19]([NH:21][C:22](=[S:23])[O:13][CH2:12][CH2:11][O:10][C:9]1[CH:14]=[CH:15][C:6]([O:5][CH2:4][CH:3]=[C:2]([CH3:16])[CH3:1])=[CH:7][CH:8]=1)[CH3:20]

Participants

4

Reactant 3

HCID 10966Ethyl isothiocyanateHCID 24758Sodium hydrideHCID 15662576HCID 15662576, compound

Product 1

HCID 19816552HCID 19816552, compound

Procedure

In the same manner, 2-[4-(3-methyl-2-butenoxy)phenoxy]-ethanol is reacted with sodium hydride and ethyl isothiocyanate to yield O-2-[4-(3-methyl-2butenoxy)phenoxy]ethyl N-ethylthiocarbamate (compound 37, Table A).

Sources & evidence

ORD record
ord-ec39510d865e4b908a301ca721f6694f
Source dataset
uspto-grants-1991_08
Patent number
US05037991

Reaction notes

Loading…