HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 14624888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | Benzenethiol, 5-amino-2-chloro-4-fluoro- | HCID 11019406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14624888 | HCID 14624888 | — |
Reaction Steps
2.00 g of 4-chloro-2-fluoro-5-mercaptoaniline was dissolved in chloroform, and 1.12 ml of thiophosgene was dropwise added at 0° C. After the dropwise addition, the temperature was raised to room temperature and then, the mixture was refluxed. After refluxing for six hours, chloroform was distilled off to obtain 2.47 g of the above-identified compound as brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05039331 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-bff620aab3b4469c86c0e4fafc68b8e4 |
| Source note | uspto-grants-1991_08 |