Propionyl chloride → HCID 14232112, compound

HRID 2248369Notes

Reaction equation

HRID 2248369 reaction equation
[N:1]1([NH:6][C:7]2[CH:12]=[CH:11][N:10]=[CH:9][CH:8]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1.C(=O)(O)[O-].[Na+].[C:18](Cl)(=[O:21])[CH2:19][CH3:20]>ClCCl>[N:10]1[CH:11]=[CH:12][C:7]([N:6]([N:1]2[CH:2]=[CH:3][CH:4]=[CH:5]2)[C:18](=[O:21])[CH2:19][CH3:20])=[CH:8][CH:9]=1

Participants

5

Reactant 3

HCID 62324Propionyl chlorideHCID 516892Sodium BicarbonateHCID 10797035HCID 10797035, compound

Product 1

HCID 14232112HCID 14232112, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent2×

Procedure

To a solution containing 2.9 g of N-(1H-pyrrol-1-yl)-4-pyridinamine and 5 g of sodium bicarbonate in 100 ml of dichloromethane was added a solution containing 1.9 g of propionyl chloride in 20 ml of dichloromethane.

Workup

  1. additionwas added a solution

Sources & evidence

ORD record
ord-af2052510756486fb5839f9ed2617a63
Source dataset
uspto-grants-1991_08
Patent number
US05039687

Reaction notes

Loading…