HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Methyl 1H-imidazole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 13655992 | HCID 13655992 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 1H-imidazole-2-carboxylate | HCID 549395 | — |
Reaction Steps
After a solution of 3.2 g (8.7 mmol.) of 1-trityl-2-carbomethoxyimidazole in 40 mL of a 5% solution of acetic acid in methanol was refluxed for 30 minutes, it was concentrated in vacuo. Recrystallization from ethanol afforded colorless needles, mp 187°-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05039691 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-3f70f74d51184acb8a75322580ecc016 |
| Source note | uspto-grants-1991_08 |