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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2248420Generated: November 3, 2026

Itaconic acid → Styrene-butadiene itaconic acid

https://huagongshe.com/reaction/2248420

Reaction equation

Participants

RoleNameHCIDCharge
ReactantItaconic acidHCID 811—
ReactantSodium PersulfateHCID 62655—
Reactant6,7-dichloro-N-cyclopentyl-4-(pyridin-4-yl)phthalazin-1-amineHCID 117072548—
SolventWaterHCID 962—
ProductStyrene-butadiene itaconic acidHCID 169127—

Reaction Conditions

Temperature150 fahrenheit

Reaction Steps

A styrene-butadiene-itaconic acid copolymer was prepared by adding to a pressure reactor with constant stirring 29.1 parts water, 1.0 parts itaconic acid, 0.5 parts of a 10 percent solution of Aerosol A-196 surfactant (sodium dicyclohexyl sulfosuccinate, available from American Cyanamid Co., Wayne, N.J.), and 0.5 parts of a polystyrene seed, 25 nm particle size. The mixture was heated to 150° F. and 0.2 parts sodium persulfate in 2.7 parts water was added to initiate the reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05039764
Source datasetuspto-grants-1991_08
ORD IDord-d2cda61ee5a34724af140b48aa1bd5f0
Source noteuspto-grants-1991_08